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Porous Nanomaterials
Science and technology
Zeolitic Framework Materials
Tuesday, 20 December 2011
A novel combined manufacturing technique for rapid production of IRMOF-1 using ultrasound and microwave energies

This Articl is published in:

Chemical Engineering Journal 165 (2010) 966–973

 by: Rana Sabouni, Hossein Kazemian, Sohrab Rohani

 

Abstract: 

 

The metal organic framework IRMOF-1 was successfully synthesized by applying a combination of ultrasonic (UTS) and microwave (MW) energy sources for rapid synthesis under various operating conditionsincluding: sonication time and temperature as well as microwave irradiation time. Moreover sample activation was employed to improve surface area of the synthesized IRMOF-1. While the highest Langmuir surface area of the as-synthesized samples was 1315m2/g sample, surface area of the activated sample was 2473m2/g. The reaction products were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), solid-state Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), and BET.

 

 

 Note: In this webloge I would like to share over two decade of my expereince in the area of zeolites sciences and technologies with you. please check the update posts. 

For further discussion, more information and references regarding any of the posts in the weblog, please contact me at : hosseinkazemian@gmail.com 


Posted by hkazemian at 12:15 PM EST
Updated: Friday, 23 December 2011 4:09 PM EST
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