A novel combined manufacturing technique for rapid production of IRMOF-1 using ultrasound and microwave energies
This Articl is published in:
Chemical Engineering Journal 165 (2010) 966–973
by: Rana Sabouni, Hossein Kazemian, Sohrab Rohani
The metal organic framework IRMOF-1 was successfully synthesized by applying a combination of ultrasonic (UTS) and microwave (MW) energy sources for rapid synthesis under various operating conditionsincluding: sonication time and temperature as well as microwave irradiation time. Moreover sample activation was employed to improve surface area of the synthesized IRMOF-1. While the highest Langmuir surface area of the as-synthesized samples was 1315m2/g sample, surface area of the activated sample was 2473m2/g. The reaction products were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), solid-state Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), and BET.
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Posted by hkazemian
at 12:15 PM EST
Updated: Friday, 23 December 2011 4:09 PM EST